Micro process engineering is approaching both academia and industry. With the provision of micro devices and systems by commercial suppliers, one main barrier for using these units has been eliminated. More and more they become familiar, thereby being one facet of the upheaval in chemical industry.
This book focuses on processes rather than on devices: what is ‘before’ and ‘behind’ micro device fabrication. A comprehensive and detailed overview is given on:
– A multi-faceted, hierarchic analysis of chemical micro process technology
– Modelling and simulation of micro reactors
– Liquid- and liquid/liquid-phase reactions
– Gas/liquid reactions
– Gas-phase reactions (heterogeneous catalysis)
Inhoudsopgave
A MULTI-FACETED, HIERARCHIC ANALYSIS OF CHEMICAL MICRO PROCESS TECHNOLOGY
Micro Reactor Differentiation and Process Intensification
Consequences of Chemical Micro Processing
Physical and Chemical Implications
Impact on Chemical Engineering
Impact on Process Engineering
Impact on Process Results
Impact on Society and Ecology
Impact on Economy
Application Fields and Markets of Micro Reactors
MODELLING AND SIMULATION OF MICRO REACTORS
Flow Phenomena on the Microscale
Methods of Computational Fluid Dynamics
Flow Distributions
Heat Transfer
Mass Transfer and Mixing
Reaction Kinetics and Modelling
Free Surface Flow
Flow in Porous Media
GAS-PHASE REACTIONS
Catalyst Coatings in Micro Channels
Micro Reactors for Gas-Phase Reactions
Oxidations
Hydrogenations
Dehydrogenations
Substitutions
Eliminations
Additions and Coupling Reactions
LIQUID- AND LIQUID/LIQUID-PHASE REACTIONS
Micro Reactors for Liquid-Phase and Liquid/Liquid-Phase Reactions
Aliphatic Nucleophilic and Electrophilic Substitution such as Esterification, Acylation of Amines, Thiocyanation, and much more
Aromatic Electrophilic and Nucleophilic Substitution such as Nitrations, Amino-de-halogenations, Diazo Chemistry, and much more
Metal-catalyzed Aromatic Substitution such as Suzuki and Sonogashira Couplings, and more
Free Radical Substitution such as Alkane Nitration
Addition to Carbon-Carbon and Carbon-hetero Multiple Bonds such as the Michael Addition, the Diels-Alder-Reaction, the Aldol Reaction, and much more
Oxidations and Reductions
Eliminations and Rearrangements
Inorganic Reactions such as the Belousov-Zhabotinskii-Reaction, Complex Formations, and much more
GAS/LIQUID CONTACTING
Micro Reactors for Gas/Liquid Contacting
Aromatic Electrophilic Substitution such as Direct Fluorinations
Free Radical Substitution such as Alkane Fluorinations and Chlorinations
Addition to Carbon-Carbon and Carbon-hetero Multiple Bonds such as Nitro-group Hydrogenation, Cycloalkane Hydrogenation, and more
Oxidations and Reductions such as Alcohol Oxidation, Photo Diels-Alder Reactions, and more
Inorganic Reactions such as Sulfite Oxidation
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