Discover new keys to solving analytical problems using the Latest sample preparation methods
Commonly viewed of as a routine task rather than as an integral component in the analytical process, sample preparation has long been undervalued as a science and underdeveloped as a technology. In an effort to reverse this trend, Handbook of Sample Preparation shows why sample preparation deserves closer scientific scrutiny, and makes a compelling case for colleges and professional laboratories to devote more resources to promote the benefits of its correct application.
Handbook of Sample Preparation includes:
- A solid overview of standard sampling methodologies and their analytical capabilities
- An introduction of non-traditional sampling technologies, which address the need for solvent-free alternatives, automation, and miniaturization
- A discussion of the analytical shift toward performing sampling on-site, rather than in the laboratory
- An examination of various extraction technologies and their applications for different types of matrices
- A look at how to take advantage of new sampling strategies to streamline laboratory procedures, reduce research costs, and increase overall productivity
An excellent primer on the fundamentals of extraction as well as a sound guide on the latest technological upgrades influencing current sampling techniques, this versatile text serves as an important and accessible tool for both students and seasoned practitioners as they seek new avenues for improving the accuracy of their analyses.
Spis treści
Preface vii
Contributors ix
Part I Fundamental Extraction Techniques 1
1 Theory of Extraction 3
Janusz Pawliszyn
2 Headspace Gas Chromatography 25
Zelda E. Penton
3 Liquid–Liquid Extraction in Environmental Analysis 39
Toh Ming Hii and Hian Kee Lee
4 Solid-Phase Extraction 53
Ronald E. Majors
5 Solid-Phase Microextraction 81
Sanja Risticevic, Dajana Vuckovic, and Janusz Pawliszyn
6 Microdialysis Sampling as a Sample Preparation Method 103
Pradyot Nandi and Susan M. Lunte
7 Liquid-Phase Microextraction (LPME) Utilizing Porous Hollow Fibers 125
Stig Pedersen-Bjergaard, Knut Einar Rasmussen, and Jan Åke Jönsson
8 Sample Preparation in Membrane Introduction Mass Spectrometry 149
Raimo A. Ketola, Tapio Kotiaho, and Frants R. Lauritsen
9 Pressurized Fluid Extraction 163
John R. Dean and Renli Ma
10 Superheated Water Extraction 181
Roger M. Smith
11 Supercritical Fluid Extraction 191
Jeremy J. Kroon and Douglas E. Raynie
12 Microwave-Assisted Extraction 197
J.R. Jocelyn Paré and Jacqueline M.R. Bélanger
13 Chemical Derivatizations in Analytical Extractions 225
Jack Rosenfeld
Part II Application Considerations 247
14 Sample Preparation Techniques for Environmental Organic Pollutant Analysis 249
Ray E. Clement and Chunyan Hao
15 Sample Preparation for the Study of Flavor Compounds in Food 267
Henryk H. Jeleń
16 Sampling and Sample Preparation for Clinical and Pharmaceutical Analysis 285
Hiroyuki Kataoka, Keita Saito, and Atsushi Yokoyama
17 Statistics of Sampling and Sample Preparation 313
Byron Kratochvil
18 SPME Devices Integrating Sampling with Sample Preparation for On-Site Analysis 325
Gangfeng Ouyang
Part III Recent Developments 341
19 Developments in the Use of Passive Sampling Devices for Monitoring Pollutants in Water 343
Graham A. Mills, Rocio Aguilar-Martínez, Richard Greenwood, Ian J. Allan, Janine Brümmer, Jesper Knutsson, and Branislav Vrana
20 Solid-Phase Microextraction for Drug Analysis 365
Heather L. Lord
21 Sample Handling Protocols for Biosensor Applications 385
Andrew Chan, Teresa Artuso, and Ulrich J. Krull
22 Sol-Gel Coatings and Monoliths in Analytical Sample Preparation 419
Scott Segro and Abdul Malik
23 The Use of Molecularly Imprinted Polymers for Sampling and Sample Preparation 445
Börje Sellergren and Antonio Martin Esteban
Index 475
O autorze
JANUSZ PAWLISZYN, Ph D, is a Professor in the Department of Chemistry at the University of Waterloo in Ontario, Canada. He is the author of
Solid Phase Microextraction (Wiley) and
Sampling and Sample Preparation in Field and Laboratory, and has been published in more than four hundred scientific publications.
HEATHER L. LORD, Ph D, is a Research Associate for New Analytical Methods and Technologies in the Department of Chemistry at the University of Waterloo. She received her Ph D in 2005 under Dr. Pawliszyn.
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