William Henderson & J. Scott McIndoe 
Mass Spectrometry of Inorganic and Organometallic Compounds [PDF ebook] 
Tools — Techniques — Tips

This is the first modern book to treat inorganic and organometallic
mass spectrometry simultaneously. It is textbook and handbook in
one; as a textbook it introduces the techniques and gives hints on
how to apply the various techniques, as a handbook it lists all
available ionization techniques for just about any given compound.
The book also includes non-mathematical explanations of how modern
MS instruments work
Mass Spectrometry of Inorganic and Organometallic
Compounds will inspire the synthetic inorganic and
organometallic chemist with the confidence to apply some of the new
techniques to their characterization problems.

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