The state-of-the-art in NMR spectral analysis.
This interactive tutorial provides readers with a comprehensive range of software tools and techniques, as well as the necessary theoretical knowledge required to analyze their spectra and obtain the correct NMR parameters.
Modern Spectral Analysis provides expert guidance, by presenting efficient strategies to extract NMR parameters from measured spectra. A database of selected spectra and modern, powerful WIN-NMR software designed by Bruker are provided on the enclosed CD-ROM. The programs provided are 1 D WIN-NMR, WIN-DAISY, WIN-DR and WIN-DYNAMICS, and direct data exchange between all these programs is possible. Readers are shown how they can obtain maximum structural information from their 1 D NMR spectra with time-saving computer assistance. Practical problems that can occur and their solutions are discussed at length using clear, easy-to-follow examples. Both homo- and heteronuclear and first- and second-order spin systems are demonstrated. Moreover, relaxation analysis, nuclear Overhauser effects and magnetic site exchange are all covered in this hands-on guide to NMR spectral analysis.
Зміст
INTRODUCTION
Scope and Audience
Organization
Personal Qualifications
Contents
Technical Requirements
Software
GENERAL CHARACTERISTICS OF SPIN SYSTEMS
The Chemical Shift
First Order Spin Systems
Second Order Spin Systems
Magnetic Equivalence
STRUCTURE AND SPIN SYSTEM PARAMETERS
Symmetry Effects
Configuration Isomers in NMR
Conformation and NMR
SPIN SYSTEMS AND THE PERIODIC TABLE
Spin-1/2 Pure Elements
Spin-1/2 Rare Isotopes
Spin Systems with Quadrupolar Nuclei
TIME DEPENDENT PHENOMENA
Relaxation Times
Nuclear Overhauser Effect
Magnetic Site Exchange
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